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Francis Rouessac - Chemical Analysis

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Название:
Chemical Analysis
Автор:
Francis Rouessac
Жанр:
unrecognised / на английском языке
Год:
неизвестен
ISBN:
нет данных
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Chemical Analysis: краткое содержание, описание и аннотация

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The new edition of the popular introductory analytical chemistry textbook, providing students with a solid foundation in all the major instrumental analysis techniques currently in use The third edition of
provides an up-to-date overview of the common methods used for qualitative, quantitative, and structural chemical analysis. Assuming no background knowledge in the subject, this student-friendly textbook covers the fundamental principles and practical aspects of more than 20 separation and spectroscopic methods, as well as other important techniques such as elemental analysis, electrochemistry and isotopic labelling methods.
Avoiding technical complexity and theoretical depth, clear and accessible chapters explain the basic concepts of each method and its corresponding instrumental techniques—supported by explanatory diagrams, illustrations, and photographs of commercial instruments. The new edition includes revised coverage of recent developments in supercritical fluid chromatography, capillary electrophoresis, miniaturized sensors, automatic analyzers, digitization and computing power, and more. Offering a well-balanced introduction to a wide range of analytical and instrumentation techniques, this textbook:
Provides a detailed overview of analysis methods used in the chemical and agri-food industries, medical analysis laboratories, and environmental sciences Covers various separation methods including chromatography, electrophoresis and electrochromatography Describes UV and infrared spectroscopy, fluorimetry and chemiluminescence, x-ray fluorescence, nuclear magnetic resonance and other common spectrometric methods such atomic or flame emission, atomic absorption and mass spectrometry Includes concise overview chapters on the general aspects of chromatography, sample preparation strategies, and basic statistical parameters Features examples, end-of-chapter problems with solutions, and a companion website featuring PowerPoint slides for instructors
, is the perfect textbook for undergraduates taking introductory courses in instrumental analytical chemistry, students in chemistry, pharmacy, biochemistry, and environmental science programs looking for information on the techniques and instruments available, and industry technicians working with problems of chemical analysis.
Review of Second Edition “An essential introduction to a wide range of analytical and instrumentation techniques that have been developed and improved in recent years.”
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17 Chapter 17Figure 17.1 Radioimmunology testing – the different steps.Figure 17.2 HPLC/MS measurement of caffeine by isotopic dilution. The stable...Figure 17.3 Different parts of an accelerator mass spectrometer (AMS).Figure 17.4 The different steps of an ELISA‐type immune‐enzymatic test with ...Figure 17.5 Relationship between concentration and absorbance of ELISA assay...Figure 17.6 The EMIT technique. Enzymes are often used as tracers because th...Figure 17.7 Diagram of neutron activation. When a neutron interacts with the...Figure 17.8 A nonconventional application of neutron activation. When it is ...Figure 17.9 Three molecules labelled at a single site with 14C. This radiois...Figure 17.10 Three molecules labelled at a single site with 14C. Fluorescenc...

18 Chapter 18Figure 18.1 Presentation of an elemental analysis.Figure 18.2 Pregl and Simon methods of microanalysis. Generations of student...Figure 18.3 Microanalysis apparatus with chromatographic detection. The fill...Figure 18.4 Instrument for nitrogen analysis. This instrument is a modern ad...Figure 18.5 A total nitrogen analyser. Model COT/TNAmong others this typ...Figure 18.6 Mercury analysers using AAS or cold vapour AFS. (a) Atomic absor...Figure 18.7 Ion mobility spectrometer (IMS). Ions are repetitively admitted ...

19 Chapter 19Figure 19.1 Measurement set‐up of an ion‐selective electrode (ISE). The sele...Figure 19.2 Glass electrode for measuring pH. The concentration of H +ions i...Figure 19.3 Measurement set‐up of ion‐specific electrodes (ISE). Diagram of ...Figure 19.4 Liquid membrane electrode for the Ca 2+ion and organic compounds...Figure 19.5 Dissolved gas potentiometric sensor. Diagrams with two separate ...Figure 19.6 Example of an assay by direct potentiometry. The calibration cur...Figure P19.1

20 Chapter 20Figure 20.1 Assembly of a voltammetric cell. (a) DC set‐up in which no curre...Figure 20.2 Evolution of the mercury drop diameter over time. Fresh‐drop DME...Figure 20.3 A polarographic wave. Polarogram of a solution containing 10 ppm...Figure 20.4 Sampling polarography. This technique increases the sensitivity ...Figure 20.5 Pulse polarography. NPP and DPP techniques. The diagram of the t...Figure 20.6 Square wave polarography (SWP). A periodic square wave signal wi...Figure 20.7 Determination of cations with a mercury film electrode by anodic...Figure 20.8 Coulometer to determine water content in accordance with the Kar...Figure 20.9 Karl Fischer coulometer electrodes. The purpose of the diaphragm...Figure 20.10 Voltammetric detection in HPLC and HPCE. (a) Two models of volt...Figure 20.11 A Clark sensor for oxygen determination. Cell with two concentr...Figure 20.12 Amperometric gas sensors (AGS).Figure 20.13 Two‐electrode cell for oxygen. The lead anode is progressively ...Figure 20.14 Two‐ and three‐electrode cells for carbon monoxide. Electrochem...Figure 20.15 Oxidation of glucose by glucose oxidase. The reaction diagram s...Figure 20.16 Amperometric measurement of glucose. First generation based on ...

21 Chapter 21Figure 21.1 Statistics displaying the proportion of time spent in each stage...Figure 21.2 Solid phase extraction. The separation of an analyte from the ma...Figure 21.3 Principle of immuno‐affinity extraction. The different steps of ...Figure 21.4 Micro‐extraction procedures. (a) Micro‐extraction using an adsor...Figure 21.5 Gas extraction. Principle of a gas/solid extraction column. A ch...Figure 21.6 Headspace analysis in static mode and in dynamic mode. In static...Figure 21.7 Supercritical fluid extraction. Comparison of the eluting powers...Figure 21.8 Microwave digester. Detailed view of the 15‐count carrousel and ...

22 Chapter 22Figure 22.1 Graphic illustration of the data from Table 22.1. To illustrate ...Figure 22.2 Gaussian curves. When the number of measurements increases and i...Figure 22.3 Linear regression and Theil’s line corresponding to the data fro...Figure 22.4 Diagram of the linear equation calculation using Theil’s method ...Figure 22.5 The one‐factor‐at‐a‐time method. If there is a continuous‐respon...

Guide

1 Cover Page

2 Title Page

3 Copyright Page

4 Foreword

5 About the companion website

6 Introduction

7 Table of Contents

8 Begin Reading

9 Appendix Table of Some Useful Constants

10 Bibliography

11 Index

12 Wiley End User License Agreement

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