Analytical Methods for Environmental Contaminants of Emerging Concern

88 88Rashid, A., Mazhar, S.H., Zeng, Q., Kiki, C., Yu, C., and Sun, Q. (2020). Simultaneous analysis of multiclass antibiotic residues in complex environmental matrices by liquid chromatography with tandem quadrupole mass spectrometry. J. Chromatogr. B 1145: 122103. doi: 10.1016/j.jchromb.2020.122103.

89 89Fauzan, T., Omar, T., Zaharin, A., Yuso, F., and Mustafa, S. (2017). An improved SPE-LC-MS/MS method for multiclass endocrine disrupting compound determination in tropical estuarine sediments. Talanta 173: 51–59. doi: 10.1016/j.talanta.2017.05.064.

90 90Hemström, P. and Irgum, K. (2006). Hydrophilic interaction chromatography. J. Sep. Sci. 29: 1784–1821. doi: 10.1002/jssc.200600199.

91 91 Montes, R., Aguirre, J., Vidal, X., Rodil, R., Cela, R., and Quintana, J.B. (2017). Screening for polar chemicals in water by trifunctional mixed-mode liquid chromatography-high resolution mass spectrometry. Environ. Sci. Technol. 51(11): 6250–6259. doi: 10.1021/acs.est.6b05135.

92 92Miossec, C., Mille, T., Lanceleur, L., and Monperrus, M. (2020). Simultaneous determination of 42 pharmaceuticals in seafood samples by solvent extraction coupled to liquid chromatography–tandem mass spectrometry. Food Chem. 322: 126765. doi: 10.1016/j.foodchem.2020.126765.

93 93Afsa, S., Hamden, K., Martin, P.A.L., and Mansour, H.B. (2020). Occurrence of 40 pharmaceutically active compounds in hospital and urban wastewaters and their contribution to Mahdia coastal seawater contamination. Environ. Sci. Pollut. Res. Int. 27(2): 1941–1955. doi: 10.1007/s11356-019-06866-5.

94 94Liang, Y., Liu, J., Zhong, Q., Yu, D., Yao, J., Huang, T., Zhu, M., and Zhou, T. (2019). A fully automatic cross used solid-phase extraction online coupled with ultra-high performance liquid chromatography–tandem mass spectrometry system for the trace analysis of multi-class pharmaceuticals in water samples. J. Pharm. Biomed. Anal. 174: 330–339. doi: 10.1016/j.jpba.2019.06.004.

95 95Tahrani, L., Loco, J.V., Anthonissen, R., Verschaeve, L., Mansour, H.B., and Reyns, T. (2017). Identification and risk assessment of human and veterinary antibiotics in the wastewater treatment plants and the adjacent sea in Tunisia. Water Sci. Technol. 76(11–12): 3000–3021. doi: 10.2166/wst.2017.465.

96 96Errayess, S.A., Lahcen, A.A., Idrissi, L., Marcoaldi, C., Chiavarini, S., and Amine, A. (2017). A sensitive method for the determination of Sulfonamides in seawater samples by solid phase extraction and UV–visible spectrophotometry. Spectrochim. Acta – Part A Mol. Biomol. Spectrosc. 181: 276–285. doi: 10.1016/j.saa.2017.03.061.

97 97Ngubane, N.P., Naicker, D., Ncube, S., Chimuka, L., and Madikizela, L.M. (2019). Determination of naproxen, diclofenac and ibuprofen in Umgeni estuary and seawater: A case of northern Durban in KwaZulu–Natal Province of South Africa. Reg. Stud. Mar. Sci. 29: 100675. doi: 10.1016/j.rsma.2019.100675.

98 98Omotola, E.O. and Olatunji, O.S. (2020). Quantification of selected pharmaceutical compounds in water using liquid chromatography-electrospray ionisation mass spectrometry (LC-ESI-MS). Heliyon 6(12): e05787. doi: 10.1016/j.heliyon.2020.e05787.

99 99Gago-Ferrero, P., Bletsou, A.A., Damalas, D.E., Aalizadeh, R., Alygizakis, N.A., Singer, H.P., Hollender, J., and Thomaidis, N.S. (2020). Wide-scope target screening of >2000 emerging contaminants in wastewater samples with UPLC-Q-ToF-HRMS/MS and smart evaluation of its performance through the validation of 195 selected representative analytes. J. Hazard. Mater. 387: 121712. doi: 10.1016/j.jhazmat.2019.121712.

100 100Mhuka, V., Dube, S., and Nindi, M.M. (2020). Occurrence of pharmaceutical and personal care products (PPCPs) in wastewater and receiving waters in South Africa using LC-OrbitrapTM MS. Emerg. Contam. 6: 250–258. doi: 10.1016/j.emcon.2020.07.002.

101 101Louw, S., Njoroge, M., Chigorimbo-Murefu, N., and Chibale, K. (2012). Comparison of electrospray ionisation, atmospheric pressure chemical ionisation and atmospheric pressure photoionisation for the identification of metabolites from labile artemisinin-based anti-malarial drugs using a QTRAP® mass spectrometer. Rapid Commun. Mass Spectrom. 26(20): 2431–2442. doi: 10.1002/rcm.6359.

102 102Wu, X., Conkle, J.L., and Gan, J. (2012). Multi-residue determination of pharmaceutical and personal care products in vegetables. J. Chromatogr. A 1254: 78–86. doi: 10.1016/j.chroma.2012.07.041.

103 103Kiszkiel-Taudul, I. (2021). Determination of antihistaminic pharmaceuticals in surface water samples by SPE-LC-MS/MS method. Microchem. J. 162: 105874. doi: 10.1016/j.microc.2020.105874.

104 104Duan, Y.P., Dai, C.M., Zhang, Y.L., and Chen, L. (2013). Selective trace enrichment of acidic pharmaceuticals in real water and sediment samples based on solid-phase extraction using multi-templates molecularly imprinted polymers. Anal. Chim. Acta 758: 93–100. doi: 10.1016/j.aca.2012.11.010.

105 105Ebele, A.J., Abdallah, M.A.E., and Harrad, S. (2017). Pharmaceuticals and personal care products (PPCPs) in the freshwater aquatic environment. Emerg. Contam. 3(1): 1–16. doi: 10.1016/j.emcon.2016.12.004.

106 106 Maranata, G.J., Surya, N.O., and Hasanah, A.N. (2021). Optimising factors affecting solid phase extraction performances of molecular imprinted polymer as recent sample preparation technique. Heliyon 7(1): e05934. doi: 10.1016/j.heliyon.2021.e05934.

107 107 Gosetti, F., Mazzucco, E., Gennaro, M.C., and Marengo, E. (2016). Contaminants in water: Non-target UHPLC/MS analysis. Environ. Chem. Lett. 14(1): 51–65. doi: 10.1016/S0045-6535(02)00769-5.

108 108Martínez-Piernas, A.B., Plaza-Bolaños, P., García-Gómez, E., Fernández-Ibáñez, P., and Agüera, A. (2018). Determination of organic microcontaminants in agricultural soils irrigated with reclaimed wastewater: Target and suspect approaches. Anal. Chim. Acta 1030: 115–124. doi: 10.1016/j.aca.2018.05.049.

109 109 Le-Minh, N., Stuetz, R.M., and Khan, S.J. (2012). Determination of six sulfonamide antibiotics, two metabolites and trimethoprim in wastewater by isotope dilution liquid chromatography/tandem mass spectrometry. Talanta 89: 407–416. doi: 10.1016/j.talanta.2011.12.053.

110 110 Hug, C., Ulrich, N., Schulze, T., Brack, W., and Krauss, M. (2014). Identification of novel micropollutants in wastewater by a combination of suspect and nontarget screening. Environ. Pollut. 184: 25–32. doi: 10.1016/j.envpol.2013.07.048.

111 111 Zhou, W., Yang, S., and Wang, P.G. (2017). Matrix effects and application of matrix effect factor. Bioanalysis 9(23): 1839–1844. doi: 10.4155/bio-2017-0214.

112 112Ho, Y.B., Zakaria, M.P., Latif, P.A., and Saari, N. (2014). Occurrence of veterinary antibiotics and progesterone in broiler manure and agricultural soil in Malaysia. Sci. Total Environ. 488–489(1): 261–267. doi: 10.1016/j.scitotenv.2014.04.109.

113 113Wu, X.L., Xiang, L., Yan, Q.Y., Jiang, Y.N., Li, Y.W., Huang, X.P., Li, H., Cai, Q.Y., and Mo, C.H. (2014). Huang, Distribution and risk assessment of quinolone antibiotics in the soils from organic vegetable farms of a subtropical city, Southern China. Sci. Total Environ. 487(1): 399–406. doi: 10.1016/j.scitotenv.2014.04.015.

114 114Choi, J.H., Lamshöft, M., Zühlke, S., Abd El-Aty, A.M., Rahman, M.M., Kim, S.W., Shim, J.H., and Spiteller, M. (2014). Analyses and decreasing patterns of veterinary antianxiety medications in soils. J. Hazard. Mater. 275: 154–165. doi: 10.1016/j.jhazmat.2014.05.005.

115 115Dodgen, L.K., Li, J., Wu, X., Lu, Z., and Gan, J.J. (2014). Transformation and removal pathways of four common PPCP/EDCs in soil. Environ. Pollut. 193: 29–36. doi: 10.1016/j.envpol.2014.06.002.

116 116Mijangos, L., Bizkarguenaga, E., Prieto, A., Fernández, L.A., and Zuloaga, O. (2015). Simultaneous determination of a variety of endocrine disrupting compounds in carrot, lettuce and amended soil by means of focused ultrasonic solid-liquid extraction and dispersive solid-phase extraction as simplified clean-up strategy. J. Chromatogr. A 1389: 8–1318. doi: 10.1016/j.chroma.2015.02.036.