Tony Waters - Process Gas Chromatographs

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A guide to the fundamentals of applied gas chromatography and the process gas chromatograph, with practical procedures for design and troubleshooting This comprehensive resource provides the theory that underpins a full understanding of the fundamental techniques of gas chromatography and the process analyzer. Without relying on complex mathematics, the book addresses hands-on applications of gas chromatographs within process industries. The author – a noted expert on the topic – details both the scientific information needed to grasp the material presented and the practical applications for professionals working in the field.
Process Gas Chromatographs:
Fundamentals, Design and Implementation
Describes practical procedures for design and troubleshooting Contains concise chapters that provide a structured course for advanced students in process engineering Reviews the fundamentals of applied gas chromatography Details the operation and maintenance of process gas chromatographs Offers a summary, and self-assessment questions, for every chapter Is written by an international expert in the field with extensive industry knowledge and teaching experience in courses on process sampling systems and gas chromatography Written for process analyzer engineers and technicians, application engineers, and industrial environmental engineers, offers an essential guide to the basics of gas chromatography and reviews the applications of process gas chromatographs in industry today.

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Dr Daniel Kuehne Process Gas Chromatograph Consultant Siemens AG Analytical - фото 9

Dr. Daniel Kuehne

Process Gas Chromatograph Consultant

Siemens AG

Analytical Products and Solutions

Manufacturing Karlsruhe, Germany

Daniel studied Chemistry at the University of Bremen and did his diploma and doctorate thesis in Analytical Chemistry.

He joined Siemens in 2005 as method developer for process GCs. He stayed in method development for 11 years, whereof the last five years being the head of the PGC method developer team.

Since 2016 he has been making technical evaluations of PGC inquiries and working as a technical consultant for sales and customers and additionally as technical advisor for the GC method development team.

Daniel has 14 years of experience working with process gas chromatographs.

James Leonard PhD Process Analyzer Specialist Eastman Chemical Company - фото 10

James Leonard, PhD

Process Analyzer Specialist

Eastman Chemical Company

Kingsport, Tennessee, USA

James received his PhD in Analytical Chemistry from The Ohio State University. He has 20 years of experience working in the field of Process Analytics at Eastman Chemical. During this time, James has designed, installed, and commissioned analyzer systems incorporating modern on‐line techniques throughout the world.

He has presented lectures on process analytics at universities and other organizations to promote the use of on‐line technologies to improve process control and reduce waste.

James has 17 years of experience working with process gas chromatographs.

Harald Mahler Process Analyzer Engineer Siemens AG Analytical Products and - фото 11

Harald Mahler

Process Analyzer Engineer

Siemens AG

Analytical Products and Solutions

Karlsruhe, Germany

Harald studied chemistry at the University of Applied Science in Reutlingen. Since 1989 he has gained experience in process analytics in various engineering and management positions within Siemens AG. He has authored and presented many technical papers within the process analytical community.

Harald has held engineering and management roles in application and method development, project management, industry marketing, and product management. Currently he is Global Sales and Business Development Manager for process analytics within the Process Automation Division, serving mainly the petrochemical, oil and gas, and renewable energy markets.

Harald has 29 years of experience working with process gas chromatographs.

Gen Matsuno ME Product Manager Quality Analyzer Systems General Manager IAPS - фото 12

Gen Matsuno, ME

Product Manager

Quality Analyzer Systems

General Manager

IA‐PS Analyzer Center

Yokogawa Electric Corporation

Mitaka, Tokyo, Japan

Matsuno‐san was leader of the Yokogawa GC8000 PGC development team. In addition to his experience of designing process gas chromatographs, he has five years of experience as a laboratory GC user.

Gen‐san has 12 years of experience working with process gas chromatographs.

Takashi Matsuura BE Senior Field Engineer Nippon Swagelok FST Inc Yokohama - фото 13

Takashi Matsuura, BE

Senior Field Engineer

Nippon Swagelok FST, Inc.

Yokohama, Japan

Formerly, Manager of Process GC Development

Yokogawa Electric Corporation

Taka designed the Yokogawa GC1000 PGC oven and was leader of the engineering team that developed the Yokogawa GC1000 Mk2 PGC. He also wrote the specifications for the GC8000 PGC.

Taka has over 25 years of experience working with process gas chromatographs.

Suru Patel PhD Process Analyzer Consultant Patex Controls Ltd Calgary - фото 14

Suru Patel, PhD

Process Analyzer Consultant

Patex Controls Ltd.

Calgary, Alberta, Canada

Formerly, Distinguished Engineering Associate for Process Analyzers

Exxon Chemical Company, Sarnia, Canada, and Singapore

In addition to his process analyzer engineering work, Suru developed PGC training courses for process analyzer technicians and PGC data users.

Previously, for several years, Suru was a PGC Applications Engineer at Servomex Company in the UK and was the Lead Analyzer Engineer in Houston for Exxon's Singapore Chemical Complex project. He was also the development engineer for a new flame ionization detector.

Suru has 40 years of experience working with process gas chromatographs.

Ivan Rybár PhD Head of Process Analyzer Group Slovnaft MaO as Bratislava - фото 15

Ivan Rybár, PhD

Head of Process Analyzer Group

Slovnaft MaO, a.s.

Bratislava, Slovakia

Formerly Research and Teaching Assistant, Department of Analytical Chemistry, Comenius University

Bratislava, Slovakia

For 10 years now, Ivan has been responsible for the reliability of all process analyzers at the refinery, including the maintenance of existing systems and the design of new installations. As the supervisor of 26 analyzers, he creates work procedures and provides training and support for his team.

In 2013 and 2015, he was twice awarded the accolade “Slovnaft Star.”

Previously he worked as an analyzer engineer for several companies providing engineering services to industrial plants, including the selection of analyzers and the design of complete sampling systems.

During his time at university, Ivan developed new methods and taught several graduate courses in liquid chromatography. He has recently published four scientific papers on this work.

Ivan has 15 years of experience working with process gas chromatographs.

Eric Schmidt PhD Principal Research Scientist The Dow Chemical Company - фото 16

Eric Schmidt, PhD

Principal Research Scientist

The Dow Chemical Company

Analytical Sciences

Freeport, Texas, USA

Eric Schmidt received his PhD in Analytical Chemistry from The University of Texas at Austin. He has worked at the Dow Chemical Company in Freeport, Texas, for over 20 years as a Research Scientist where he spends his time developing new on‐line process measurements for R&D and manufacturing. He is currently leading the On‐line Chromatography Strategic Capability Team at Dow.

Eric has 20 years of experience working with process gas chromatographs.

Acknowledgments

Hearty thanks all friends and associates who contributed material to this text. Many of those listed below audited the beta‐test of an online tutorial based on this textbook. Their contributions of time and knowledge are much appreciated.

Minh Anh Vietnam
Brian Aplin South Carolina
Dale Arstein Ohio
Masafumi Awano Japan
Ken Backus Texas
Hesham El Banna Saudi Arabia
Eddie Beezemer Netherlands
Linda Bonnette Texas
Mark Booth Scotland
Danny van den Burg Netherlands
Bruno Chaurand France
Alice Chin Malaysia
Alex Chu England
Scott Cookson Australia
Marcus Creaven Ireland
Dave Demsey Sr. Pennsylvania
Matt Dixon Ohio
Ana Dominguez Switzerland
Kevin Fajri Indonesia
Mikhail Fedorets Russia
Mike Frost Australia
Victor Alberto Fuentes Spain
Keisuke Fukada Japan
Yves Gamache Quebec
Udo Gellert Germany
Roger Glass England
Urich Gokeler Texas
Matt Hasenohr Oregon
Darryl Hazlett Texas
Jack Holland England
Tom Huddle England
Damian Huff West Virginia
Humberto Serrato Hurtado Colombia
Joe Iveljic Ohio
Nick Iverson Minnesota
Samson Jacob Abu Dhabi
Jayson Zhang Ji Singapore
Kyle Juist Ohio
Eric Kayla California
Eric Kvarda Ohio
Bert Laan England
André Lamontagne Quebec
Wilco Landkroon Netherlands
Rudi Lehnig Germany
Tim Lenior Netherlands
Hank Liu Singapore
Aldemar Figueroa Loza Colombia
Karim Mahraz Ohio
Rogério Matos Brazil
Bill Menz Ohio
John Meyer Germany
Thomas Neuhauser Oklahoma
Kentaro Nomura Japan
Doug Nordstrom Ohio
Tatsuya Ohkoshi Japan
Bob Perusek Ohio
Stacey Phillips Alberta
Wouter Pronk Netherlands
Venkat Rao Dubai, UAE
Syed Jawwad Raza Qatar
Reino van Rensburg South Africa
Joe Rodriguez Ohio
Zaffar Shariff Singapore
Joel Siallagan Indonesia
Trey Sinkfield Texas
Charlie Smith Louisiana
Sharon Sng Singapore
Mike Strobel Pennsylvania
Max Sukuma Australia
Asad Tahir Texas
Jorge Trillos Colombia
Steve Trimble Oklahoma
Kunawat Wattanakij Thailand
Mark Welch England
Henk van Well Germany
Martin Wieser Germany
Kenta Yamada Japan
Norbert Zeug Germany

Part One PGC fundamentals

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