H. L. Li - Organic Structures from Spectra

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The derivation of structural information from spectroscopic data is now an integral part of organic chemistry courses at all Universities. A critical part of any such course is a suitable set of problems to develop the students’ understanding of how organic structures are determined from spectra. The book builds on the very successful teaching philosophy of learning by hands-on problem solving; carefully graded examples build confidence and develop and consolidate a student’s understanding of organic spectroscopy.
Organic Structures from Spectra, 6th Edition 
The examples themselves have been selected to include all important structural features and to emphasise connectivity arguments and stereochemistry. Many of the compounds were synthesised specifically for this book. In this collection, there are many additional easy problems designed to build confidence and to demonstrate basic principles.
The Sixth Edition now incorporates many new problems using 2D NMR spectra (C–H Correlation spectroscopy, HMBC, COSY, NOESY and TOCSY); has been expanded and updated to reflect the new developments in NMR spectroscopy; has an additional 40 carefully selected basic problems; provides a set of problems dealing specifically with the quantitative analysis of mixtures using NMR spectroscopy; features proton NMR spectra obtained at 200, 400 and 600 MHz and 13C NMR spectra including routine 2D C–H correlation, HMBC spectra and DEPT spectra; contains a selection of problems in the style of the experimental section of a research paper; includes examples of fully worked solutions in the appendix; has a complete set of solutions available to instructors and teachers from the authors.
will prove invaluable for students of Chemistry, Pharmacy and Biochemistry taking a first course in Organic Chemistry.

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Organic Structures from Spectra

Sixth Edition

L. D. Field

Professor of Chemistry

School of Chemistry

University of New South Wales, Australia

H. L. Li

Senior Research Associate

School of Chemistry

University of New South Wales, Australia

A. M. Magill

Honorary Research Associate

School of Chemistry

University of New South Wales, Australia

This edition first published 2020 2020 John Wiley Sons Ltd Edition History - фото 1

This edition first published 2020

© 2020 John Wiley & Sons Ltd

Edition History

John Wiley & Sons (4e, 2008)

John Wiley & Sons (5e, 2013)

All rights reserved. No part of this publication may be reproduced, stored in a retrieval system, or transmitted, in any form or by any means, electronic, mechanical, photocopying, recording or otherwise, except as permitted by law. Advice on how to obtain permission to reuse material from this title is available at http://www.wiley.com/go/permissions.

The right of L. D. Field, H. L. Li and A. M. Magill to be identified as the authors of this work has been asserted in accordance with law.

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In view of ongoing research, equipment modifications, changes in governmental regulations, and the constant flow of information relating to the use of experimental reagents, equipment, and devices, the reader is urged to review and evaluate the information provided in the package insert or instructions for each chemical, piece of equipment, reagent, or device for, among other things, any changes in the instructions or indication of usage and for added warnings and precautions. While the publisher and authors have used their best efforts in preparing this work, they make no representations or warranties with respect to the accuracy or completeness of the contents of this work and specifically disclaim all warranties, including without limitation any implied warranties of merchantability or fitness for a particular purpose. No warranty may be created or extended by sales representatives, written sales materials or promotional statements for this work. The fact that an organization, website, or product is referred to in this work as a citation and/or potential source of further information does not mean that the publisher and authors endorse the information or services the organization, website, or product may provide or recommendations it may make. This work is sold with the understanding that the publisher is not engaged in rendering professional services. The advice and strategies contained herein may not be suitable for your situation. You should consult with a specialist where appropriate. Further, readers should be aware that websites listed in this work may have changed or disappeared between when this work was written and when it is read. Neither the publisher nor authors shall be liable for any loss of profit or any other commercial damages, including but not limited to special, incidental, consequential, or other damages.

Library of Congress Cataloging-in-Publication Data

Names: Field, L. D., author.

Title: Organic structures from spectra / L.D. Field, Professor of

Chemistry, School of Chemistry, University of New South Wales, H.L.

Li, Senior Research Fellow, School of Chemistry, University of New South

Wales, A.M. Magill, Honorary Research Fellow, School of Chemistry, University of New South Wales.

Description: Sixth edition. | Hoboken, NJ : Wiley, 2020. | Includes bibliographical references and index.

Identifiers: LCCN 2020004972 (print) | LCCN 2020004973 (ebook) | ISBN 9781119524809 (paperback) | ISBN 9781119524793 (adobe pdf) | ISBN 9781119524847 (epub)

Subjects: LCSH: Spectrum analysis–Problems, exercises, etc. | Organic compounds–Structure–Problems, exercises, etc.

Classification: LCC QD272.S6 S74 2020 (print) | LCC QD272.S6 (ebook) | DDC 543/.17—dc23

LC record available at https://lccn.loc.gov/2020004972

LC ebook record available at https://lccn.loc.gov/2020004973

Cover Design: Wiley

Cover Image: Courtesy of Professor L. D. Field, Dr. Hsiu Lin Li and Dr. Alison Magill; © Chernookaya/Shutterstock

PREFACE

This is the Sixth Edition of the text “Organic Structures from Spectra”. The original text, published in 1986 by J R Kalman and S Sternhell, was a remarkable instructive text at a time where spectroscopic analysis, particularly NMR spectroscopy, was becoming widespread and routinely available in many chemical laboratories. The original text was founded on the premise that the best way to learn to obtain “structures from spectra” is to build up skills by practising on simple problems. Editions two through five of the text have been published at about five-yearly intervals and each revision has taken account of new developments in spectroscopy as well as dropping out techniques that have become less important or obsolete over time. The collection has grown substantially and we are deeply indebted to Dr John Kalman and to Emeritus Professor Sev Sternhell for their commitment and contribution to all of the previous editions of “Organic Structures from Spectra”.

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